双环[2.2.2]辛烷-1,4-二羧酸二乙酯合成路线 （共 15 条）
参考文献
Guha
Chemische Berichte, 1939 , vol. 72, p. 1359,1363, 1372
反应条件
potassium hydroxide in ethanol
参考文献
Moghaddam, Sarvin; Yang, Cheng; Rekharsky, Mikhail; Ko, Young Ho; Kim, Kimoon; Inoue, Yoshihisa; Gilson, Michael K.
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3570 - 3581
反应条件
1: ethanolic KOH 2: triethylamine; chlorocarbonic acid ethyl ester; NH3 3: POCl3; 1,2-dichloro-ethane 4: ethanolic KOH View Scheme
参考文献
Roberts et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 637,639
反应条件
1: 98 percent / LiAlH4 / diethyl ether / 5 h / Heating
2: 74.2 percent / Pyridine / 48 h
3: 40 percent Spectr. / LiAlH4 / tetrahydrofuran / 21 h / Heating
View Scheme
参考文献
Kumar, Kanta; Wang, Shin Shin; Sukenik, Chaim N.
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 665 - 670
反应条件
1: 98 percent / LiAlH4 / diethyl ether / 5 h / Heating
2: 74.2 percent / Pyridine / 48 h
View Scheme
参考文献
Kumar, Kanta; Wang, Shin Shin; Sukenik, Chaim N.
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 665 - 670
