2-苯基乙基-1-硼酸频哪醇酯合成路线 （共 56 条）
反应条件
1: With potassium carbonate in methanol; toluene T=60°C; Michael type reaction; 96 h; Inert atmosphere; 2: With water; ammonium chloride in methanol; toluene Inert atmosphere;
参考文献
Cano, Rafael; Ramon, Diego J.; Yus, Miguel
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3458 - 3460
反应条件
(η-1,5-cyclooctadiene) {[4(R),5(R)]-1-benzoyl-2-[(S)-2-diphenylphosphinoferrocenyl]-4,5-diphenyl-4,5-dihydro-1-imidazole} iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in dichloromethane T=50°C; P=7500.75 Torr; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Roseblade, Stephenj.; Casas-Arce, Eva; Nettekoven, Ulrike; Gazic Smilovic, Ivana; Zanotti-Gerosa, Antonio; Casar, Zdenko
Synthesis (Germany), 2013 , vol. 45, # 20 art. no. SS-2013-Z0439-PSP, p. 2824 - 2831
反应条件
Wilkinson's catalyst in dichloromethane 25°C, 10 min;
参考文献
Crudden, Cathleen M.; Hleba, Yonek B.; Chen, Austin C.
Journal of the American Chemical Society, 2004 , vol. 126, # 30 p. 9200 - 9201
反应条件
terpyridine; [RhCl(η2:η2-cycloocta-1,5-diene)]2; sodium t-butanolate T=80°C; 24 h; Inert atmosphere;
参考文献
Gong, Tian-Jun; Jiang, Yuan-Ye; Fu, Yao
Chinese Chemical Letters, 2014 , vol. 25, # 3 p. 397 - 400
反应条件
copper(l) iodide; lithium methanolate; triphenylphosphine in N,N-dimethyl-formamide T=25°C; 18 h; Inert atmosphere;
参考文献
Yang, Chu-Ting; Zhang, Zhen-Qi; Tajuddin, Hazmi; Wu, Chen-Cheng; Liang, Jun; Liu, Jing-Hui; Fu, Yao; Czyzewska, Maria; Steel, Patrick G.; Marder, Todd B.; Liu, Lei
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 528 - 532
参考文献
Kalinin, Alexey V.; Scherer, Stefan; Snieckus, Victor
Angewandte Chemie - International Edition, 2003 , vol. 42, # 29 p. 3399 - 3404
反应条件
1: in diethyl ether T=20°C; 1 h; 2: With magnesium sulfate in diethyl ether T=20°C; 16 h;
参考文献
Hesse, Matthew J.; Butts, Craig P.; Willis, Christine L.; Aggarwal, Varinder K.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12444 - 12448
Angew. Chem., 2012 , vol. 124, # 50 p. 12612 - 12616,5
反应条件
potassium tert-butylate; copper(l) chloride in toluene 60°C, 7 h;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 33 p. 6062 - 6064
Angewandte Chemie, , vol. 121, # 33 p. 6178 - 6180
反应条件
[(2,6-(2,4,6-Me3-C6H2-NdCMe)2C5H3N)Fe(N2)]2(μ2-N2) in neat (no solvent) T=25°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 11 p. 2680 - 2683
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki coupling; 2.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Ishioka, Takafumi; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 10 p. 4826 - 4831
