间-四苯基卟吩氯化铁(III)合成路线 (共 28 条)
参考文献
Massoudipour, Morteza; Tewari, Sharad Kumar; Pandey, Krishna Kumar
Polyhedron, 1989 , vol. 8, p. 1447 - 1452
反应条件
mercury activated zinc in toluene
byproducts: ZnCl2, amalgum; (He); a mixture of Fe-complex and mercury activated zinc stirred in toluene; filtered; crystd. by addn. of heptane;
参考文献
Landrum, John T.; Hatano, K.; Scheidt, W. Robert; Reed, Christopher A.
Journal of the American Chemical Society, 1980 , vol. 102, # 22 p. 6729 - 6735
反应条件
ethanethiol in benzene
24 h;
参考文献
Li, Jianfeng; Noll, Bruce C.; Schulz, Charles E.; Scheidt, W. Robert
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5010 - 5013
Angewandte Chemie, 2009 , vol. 121, p. 5110 - 5113
反应条件
in toluene
byproducts: H2; cocondensation of iron and toluene vapor at liq. nitrogen temp.; heating to -94.6°C; dropwise addn. of porphine soln. under nitrogen to the slurry (molar ratio Fe:porphine 4:1); gradually warming to 0°C, 1h; filtration; evapn. of filtrate;
参考文献
Reagen, William K.; Radonovich, Lewis J.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5274 - 5275
参考文献
Pawlik, M. J.; Miller, P. K.; Sullivan, E. P.; Levstik, M. A.; Almond, D. A.; Strauss, S. H.
Journal of the American Chemical Society, 1988 , vol. 110, # 10 p. 3007 - 3012
反应条件
in solid
heated at 470°C at 3E-5 Torr;
参考文献
Kurtikyan, Tigran S.; Gulyan, Gurgen M.; Martirosyan, Garik G.; Lim, Mark D.; Ford, Peter C.
Journal of the American Chemical Society, 2005 , vol. 127, # 17 p. 6216 - 6224
反应条件
in deuterated toluene
byproducts: CH2CH2CH3-radical; Irradiation (UV/VIS);
参考文献
Arasasingham, Ramesh D.; Balch, Alan L.; Cornman, Charles R.; Latos-Grazynski, Lechoslaw
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4357 - 4363
反应条件
in deuterated toluene
byproducts: CH2CH3-radical; Irradiation (UV/VIS);
参考文献
Arasasingham, Ramesh D.; Balch, Alan L.; Cornman, Charles R.; Latos-Grazynski, Lechoslaw
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4357 - 4363
反应条件
in solid
heated at 470°C at 3E-5 Torr;
参考文献
Kurtikyan, Tigran S.; Gulyan, Gurgen M.; Martirosyan, Garik G.; Lim, Mark D.; Ford, Peter C.
Journal of the American Chemical Society, 2005 , vol. 127, # 17 p. 6216 - 6224
反应条件
in deuterated toluene
byproducts: CH3-radical; Irradiation (UV/VIS);
参考文献
Arasasingham, Ramesh D.; Balch, Alan L.; Cornman, Charles R.; Latos-Grazynski, Lechoslaw
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4357 - 4363