间-四苯基卟吩氯化铁(III)合成路线 （共 28 条）
反应条件
in neat (no solvent)
byproducts: pyridine; Heating at 220°C for 5 h under high vac.;
参考文献
Paeng; Nakamoto
Journal of the American Chemical Society, 1990 , vol. 112, # 9 p. 3289 - 3297
反应条件
hydroxide in pyridine; N,N-dimethyl-formamide
addition of OH(1-) to soln. of complex in mixt. of pyridine and DMF; UV, cyclic voltammetry;
参考文献
Srivatsa, G. Susan; Sawyer, Donald T.
Inorganic Chemistry, 1985 , vol. 24, p. 1732 - 1734
反应条件
in benzene
Irradiation (UV/VIS); photoexcitation (single 532 or 355-nm 25-ps FWHM pulse); determination with picosecond absorption spectroscopy, total yield no more than about 1E-4 (80percent of TPPFe(1+) and TPPFe-O(1-));
参考文献
Guest, C. R.; Straub, K. D.; Hutchinson, J. A.; Rentzepis, P. M.
Journal of the American Chemical Society, 1988 , vol. 110, # 16 p. 5276 - 5280
反应条件
zinc amalgam in toluene
stirred overnight under an argon atmosphere in a glove box; not isolated from the soln.;
参考文献
Crawford, Philip W.; Ryan, Michael D.
Inorganica Chimica Acta, 1991 , vol. 179, p. 25 - 34
反应条件
in benzene
byproducts: C6H5CH2OH, C6H5CHO; Irradiation (UV/VIS); irradiating a soln. of the complex and the substrate (350 - 420 nm, 300 W-xenon lamp, inert atmosphere);
参考文献
Suslick, Kenneth S.; Watson, Randall A.
Inorganic Chemistry, 1991 , vol. 30, p. 912 - 919
反应条件
in benzene
byproducts: C6H5CH2CHO, C6H5CHCH2O, C6H4C(O)CH3; Irradiation (UV/VIS); irradiating a soln. of the complex and the substrate (350 - 420 nm, 300 W-xenon lamp, inert atmosphere);
参考文献
Suslick, Kenneth S.; Watson, Randall A.
Inorganic Chemistry, 1991 , vol. 30, p. 912 - 919
反应条件
in benzene
byproducts: OP(C6H5)3; Irradiation (UV/VIS); irradiating a soln. of the complex and the substrate (350 - 420 nm, 300 W-xenon lamp, inert atmosphere);
参考文献
Suslick, Kenneth S.; Watson, Randall A.
Inorganic Chemistry, 1991 , vol. 30, p. 912 - 919
反应条件
in toluene
T=20°C; Inert atmosphere;
参考文献
Meininger, Daniel J.; Caranto, Jonathan D.; Arman, Hadi D.; Tonzetich, Zachary J.
Inorganic Chemistry, 2013 , vol. 52, # 21 p. 12468 - 12476
反应条件
in toluene
T=20°C; Inert atmosphere;
参考文献
Meininger, Daniel J.; Caranto, Jonathan D.; Arman, Hadi D.; Tonzetich, Zachary J.
Inorganic Chemistry, 2013 , vol. 52, # 21 p. 12468 - 12476
反应条件
in propionic acid
in situ synthesis on RB-carbon support;
参考文献
Kirschenmann; Woehrle
Berichte der Bunsengesellschaft/Physical Chemistry Chemical Physics, 1988 , vol. 92, # 11 p. 1403 - 1406
