N,N'-二甲基三亚甲基硫脲合成路线 （共 7 条）
反应条件
sulfur
T=150°C; 12 h;
参考文献
Denk, Michael K.; Gupta, Shilpi; Brownie, John; Tajammul, Sabiha; Lough, Alan J.
Chemistry - A European Journal, 2001 , vol. 7, # 20 p. 4477 - 4486
反应条件
1: With pyridine
24 h; Heating;
2: With iodine in pyridine
20 h; Heating;
参考文献
Denk, Michael K.; Gupta, Shilpi; Brownie, John; Tajammul, Sabiha; Lough, Alan J.
Chemistry - A European Journal, 2001 , vol. 7, # 20 p. 4477 - 4486
反应条件
potassium carbonate in acetonitrile
4 h; Heating;
参考文献
Bogat-skii, A. V.; Luk'yanenko, N. G.; Kirichenko, T. I.; Limich, V. V.; Nazarova, N. Yu.; Karpenko, L. P.
Journal of Organic Chemistry USSR (English Translation), 1985 , p. 1379 - 1385
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 7 p. 1513 - 1519
反应条件
1: diethyl ether
2: 91 percent / S8 / 12 h / 150 °C
View Scheme
参考文献
Denk, Michael K.; Gupta, Shilpi; Brownie, John; Tajammul, Sabiha; Lough, Alan J.
Chemistry - A European Journal, 2001 , vol. 7, # 20 p. 4477 - 4486
反应条件
bis(1,5-cyclooctadiylboryl)sulfide in 1,3,5-trimethyl-benzene
5 h; Heating;
参考文献
Koester, Roland; Kucznierz, Ralf
Liebigs Annalen der Chemie, 1992 , # 10 p. 1081 - 1086
反应条件
hydrogenchloride in ethanol
10 h; Heating; Yield given;
参考文献
Li, Chau-der; Mella, Sharon L.; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 9 p. 1089 - 1092
反应条件
T=200°C; P=1 Torr; Yield given;
参考文献
Bogatsky, A. V.; Lukyanenko, N. G.; Kirichenko, T. I.; Limich, V. V.
Synthesis, 1984 , # 2 p. 136
