3,4,7,8-四甲基-1,10-菲罗啉合成路线 （共 10 条）
反应条件
diarsenic pentoxide; sulfuric acid T=100 - 140°C;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1828
反应条件
hydrogenchloride T=80°C; 16 h;
参考文献
Butt, Graeme; Topsom, Ronald D.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 641 - 642
反应条件
1: SnCl2+2 H2O; ethanol 2: as2O5; aqueous H2SO4 / 100 - 140 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1828
反应条件
1: arsenic (V)-oxide; aqueous sulfuric acid 2: SnCl2+2 H2O; ethanol 3: as2O5; aqueous H2SO4 / 100 - 140 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1828
反应条件
1: arsenic (V)-oxide; aqueous sulfuric acid 2: SnCl2+2 H2O; ethanol 3: as2O5; aqueous H2SO4 / 100 - 140 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1828
反应条件
H2O in further solvent(s) Kinetics; aquation rate constant in triton X-100 solvent detd. by spectrophotometric measurements;
参考文献
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, , vol. 84, # 1 p. 1 - 8
反应条件
sodium sulfate in ethanol; water Reagents were mixed in water-ethanol, added satd. Na2SO4, cooled in refrigerator for 1 h;; washed with ether and suction dried;;
参考文献
Ram, M. S.; Stanbury, David M.
Journal of the American Chemical Society, 1984 , vol. 106, # 26 p. 8136 - 8142
反应条件
dihydrogen peroxide in acetic acid T=75 - 80°C; 7 h;
参考文献
Holan, George; Wernert, Gregory T.
Australian Journal of Chemistry, 1987 , vol. 40, # 5 p. 873 - 881
反应条件
CuI; caesium carbonate; benzyl alcohol in o-xylene
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
in chloroform
reagents were mixed; product was filtered off, washed with chloroform and dried in air; elem.anal.;
参考文献
Cusack, Paul A.; Patel, Bhagwati N.
Inorganica Chimica Acta, 1984 , vol. 86, p. 1 - 4
