1,2-二氢-1-苯基萘合成路线 （共 25 条）
反应条件
formic acid; sulfuric acid; dihydrogen peroxide 1.) 35 deg C, 2 h, room temp., 12 h; 2.) reflux, 10 h; Yield given. Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 5-6 p. 161 - 166
反应条件
in methanol T=-72°C; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Woning, Jan; Lijten, Frank A. T.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2427 - 2435
反应条件
propylamine Irradiation;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 109, # 3 p. 168 - 171
反应条件
T=900°C; P=0.1 Torr; flash vacuum pyrolysis; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1819 - 1828
反应条件
1: 29 percent Chromat. / 850 °C / 0.1 Torr / flash vacuum pyrolysis 2: 24 percent Chromat. / 900 °C / 0.1 Torr / flash vacuum pyrolysis; variation of reaction temperature View Scheme
参考文献
Lamberts, Joseph J. M.; Cuppen, Theo J. H. M.; Laarhoven, Wim H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1819 - 1828
反应条件
oxalic acid in water
6 h; Heating;
参考文献
Vebrel, Joel; Carrie, Robert
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 161 - 166
反应条件
tri(n-propyl)amine; Palladacycle
T=110°C; Heck reaction;
参考文献
Maeda, Kenji; Farrington, Edward J.; Galardon, Erwan; John, Benjamin D.; Brown, John M.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 104 - 109
反应条件
1: 9.2 g / H2 / palladium on charcoal / methanol / 3 h / 710 Torr
2: 7.6 g / polyphosphoric acid / 1 h / 90 °C
3: 4.8 g / sodium borohydride / ethanol
4: 70 percent / phosphoric acid / 2 h / 120 - 130 °C
View Scheme
参考文献
Kopecky, Karl R.; Hall, Michael C.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 3095 - 3104
反应条件
1: NaBH4 / methanol / 4 h / Ambient temperature
2: 87 percent / oxalic acid / H2O / 6 h / Heating
View Scheme
参考文献
Vebrel, Joel; Carrie, Robert
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 161 - 166
反应条件
in hexane
4 h; Irradiation;
参考文献
Lamberts, Joseph J. M.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1983 , vol. 48, # 13 p. 2202 - 2206
