您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
16616-42-5
合成路线
（共 31 条）
122-01-0
氯化对氯苯甲酰
+
32584-71-7
→
反应条件
16616-42-5
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane T=80°C; Substitution; 1.7 h;
参考文献
Kakusawa, Naoki; Yamaguchi, Kouichiro; Kurita, Jyoji; Tsuchiya, Takashi
Tetrahedron Letters, 2000 , vol. 41, # 21 p. 4143 - 4146
201230-82-2
+
29540-84-9
三氟甲磺酸-4-氯苯醚
+
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
[{Pd(cinnamyl)Cl}2]; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=110°C; Sonogashira coupling; P=7500.75 Torr; 2 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Sundararaju, Basker; Neumann, Helfried; Dixneuf, Pierre H.; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 1 p. 106 - 110
104-88-1
4-氯苯甲醛
+
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2 h; 2: 4-chlorobenzaldehyde in tetrahydrofuran; hexane T=0 - 20°C; 1 h; 3: With iodine; potassium carbonate in tert-butyl alcohol 3 h; Reflux;
参考文献
Ushijima, Sousuke; Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 5 p. 1436 - 1442
122-01-0
氯化对氯苯甲酰
+
159087-45-3
2-苯基-1-乙炔硼酸频那醇酯
→
反应条件
16616-42-5
反应条件
copper(l) chloride in DMI T=120°C; 0.5 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Saito, Daisuke; Inoue, Eiji; Okada, Yoshiaki; Miyazaki, Mikihiro; Inoue, Yoshiaki; Takagi, Kentaro
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 306 - 308
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
1: magnesium / diethyl ether / 0 - 20 °C 2: manganese(IV) oxide / dichloromethane / 2 h / Reflux View Scheme
参考文献
Taylor, Cassandra; Bolshan, Yuri
Organic Letters, 2014 , vol. 16, # 2 p. 488 - 491
201230-82-2
+
106-47-8
对氯苯胺
+
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in tetrahydrofuran; dimethyl sulfoxide T=32°C; Sonogashira coupling; P=7500.75 Torr; 16 h; Autoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2011 , vol. 50, # 47 p. 11142 - 11146
104-88-1
4-氯苯甲醛
→
反应条件
16616-42-5
反应条件
1: magnesium / diethyl ether / 0 - 20 °C 2: manganese(IV) oxide / dichloromethane / 2 h / Reflux View Scheme
参考文献
Chu, Xue-Ping; Zhou, Qing-Fa; Zhao, Shen; Ge, Fei-Fei; Fu, Mian; Chen, Jia-Peng; Lu, Tao
Chinese Chemical Letters, 2013 , vol. 24, # 2 p. 120 - 122
13984-49-1
+
122-01-0
氯化对氯苯甲酰
→
反应条件
16616-42-5
反应条件
palladium; triphenylphosphine in tetrahydrofuran T=50°C; Negishi Coupling; 6 h; Inert atmosphereGreen chemistry; Catalytic behavior;
参考文献
Wu, Wei-Yi; Lin, Tze-Chiao; Takahashi, Tamotsu; Tsai, Fu-Yu; Mou, Chung-Yuan
ChemCatChem, 2013 , vol. 5, # 4 p. 1011 - 1019
106-39-8
4-溴氯苯
+
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
1: caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium diacetate / dimethyl sulfoxide / 2 h / 100 °C / |Inert atmosphere 2: silica gel; water / dichloromethane / 20 °C / |Inert atmosphere View Scheme
参考文献
Tang, Ting; Fei, Xiang-Dong; Ge, Zhi-Yuan; Chen, Zhong; Zhu, Yong-Ming; Ji, Shun-Jun
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3170 - 3175
623-03-0
对氯苯甲腈
+
536-74-3
苯乙炔
→
反应条件
16616-42-5
反应条件
1.1: {(2,6-i-Pr2C6H3NC(O)Ph)Eu[N(TMS)2](THF)}2 / neat (no solvent) / 0.05 h / |Inert atmosphere; |Schlenk technique 1.2: 255 / 12 h / 20 °C / |Inert atmosphere; |Schlenk technique 2.1: sulfuric acid; water / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Ding, Hao; Lu, Chengrong; Hu, Xiaolin; Zhao, Bei; Wu, Bing; Yao, Yingming
Synlett, 2013 , vol. 24, # 10 art. no. ST-2013-W0161-L, p. 1269 - 1274
首页
上一页
1
2
3
4
下一页
末页
到第
页
确定
