反应条件
1.1: SOCl2 / benzene / 2 h / 50 - 60 °C
2.1: 91 percent / benzene; pyridine / 20 °C
3.1: 85 percent / POCl3 / toluene / 3 h / Heating
4.1: 92 percent / methylene blue; O2 / CH2Cl2; methanol / 0.5 h / 15 °C / Irradiation
5.1: 82 percent / acetonitrile / 1.25 h / Heating
6.1: 92 percent / H2 / PtO2 / methanol / 3 h / 17 °C
7.1: 90 percent / NaBH4 / methanol / 2 h
8.1: CuCl2 / toluene / 0.03 h / 140 °C
8.2: NaBH4 / methanol / 2 h / 20 °C
View Scheme
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Kanbayashi, Ryo; Tokuda, Masao; Suginome, Hiroshi
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6583 - 6596
