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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
16620-96-5
合成路线
（共 76 条）
120-14-9
3,4-二甲氧基苯甲醛
→
反应条件
16620-96-5
反应条件
1: AcOH / ethanol / 20 h / Heating 2: NaBH4 / methanol / 1 h / Ambient temperature 3: 98 percent / Ac2O / 1 h / 70 °C 4: 96 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 5: 97 percent / TFAA / benzene / 20 h / Ambient temperature 6: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 7: 87 percent / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
121580-32-3
→
反应条件
16620-96-5
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Heating;
参考文献
Takano, Seiichi; Iida, Hirokazu; Inomata, Kohei; Ogasawara, Kunio
Heterocycles, 1993 , vol. 35, # 1 p. 47 - 52
74046-23-4
→
反应条件
16620-96-5
反应条件
sodium tetrahydroborate in methanol Yield given;
参考文献
Knabe; Grunewald
Archiv der Pharmazie, 1987 , vol. 320, # 6 p. 492 - 499
1745-07-9
6,7-二甲氧基-1,2,3,4-四氢异喹啉
+
74-88-4
甲基碘
→
反应条件
16620-96-5
反应条件
in ethyl acetate T=0 - 20°C;
参考文献
Molander, Gary A.; Pack, Shawn K.
Tetrahedron, 2003 , vol. 59, # 52 p. 10581 - 10591
191545-70-7
→
反应条件
16620-96-5
反应条件
1: 96 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 2: 97 percent / TFAA / benzene / 20 h / Ambient temperature 3: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 4: 87 percent / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
191545-89-8
→
反应条件
16620-96-5
反应条件
1: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 2: 87 percent / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
191545-76-3
→
反应条件
16620-96-5
反应条件
1: 97 percent / TFAA / benzene / 20 h / Ambient temperature 2: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 3: 87 percent / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
191545-69-4
→
反应条件
16620-96-5
反应条件
1: 93 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 2: 64 percent / TFAA / benzene / 16 h / Ambient temperature 3: 59 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 4: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
191545-74-1
→
反应条件
16620-96-5
反应条件
1: 64 percent / TFAA / benzene / 16 h / Ambient temperature 2: 59 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 3: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
191545-88-7
→
反应条件
16620-96-5
反应条件
1: 59 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 2: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
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