反应条件
1: 73.4 percent / CH2Cl2 / 1.5 h / 0 °C
2: 2.) 55percent aq. HI / 1.) aq. ethanol, 0 deg C, 20 min, 2.) ethanol
3: 57 percent / sodium borohydride / ethanol / 0.75 h
4: 1.) sodium hydride / 1.) THF, 1.5 h, 2.) 15 min
5: 73.8 percent / acetone / 69 h / Heating
6: 2.) sodium borohydride / 1.) methanol, irradiation, 3 h, 2.) 98percent aq. EtOH, heating
View Scheme
参考文献
Hutchins, Michael; Sainsbury, Malcolm; Scopes, David I. C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2059 - 2064
