2-氨基-3-甲基-5-碘吡啶合成路线 (共 6 条)
反应条件
copper(l) iodide; N,N,N',N',tetramethyl-ethylenediamine; sodium iodide in 1,4-dioxane T=110°C;
参考文献
US2006/69093 A1, ;
Page/Page column 23 ;
US 20060069093 A1
反应条件
sulfuric acid; iodine; periodic acid in acetic acid T=80°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5356 - 5359
反应条件
1: With sulfuric acid; sodium nitrite T=60°C; 0.25 h; 2: With boric acid in water T=0 - 100°C;
参考文献
Lan, Tao; McLaughlin, Larry W.
Journal of the American Chemical Society, 2000 , vol. 122, # 27 p. 6512 - 6513
反应条件
hydrogen bromide; bromine; sodium nitrite T=0°C; 0.5 h;
参考文献
Hsieh; McLaughlin
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5356 - 5359
反应条件
chlorine; sodium nitrite in water
参考文献
BASF Aktiengesellschaft
Patent: US6372766 B1, 2002 ;
反应条件
in ethanol; water
24 h; Heating;
参考文献
Veron, Jean-Baptiste; Enguehard-Gueiffier, Cecile; Snoeck, Robert; Andrei, Graciela; De Clercq, Erik; Gueiffier, Alain
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 22 p. 7209 - 7219