1-氨基环戊烷-1-羧酸乙酯合成路线 （共 18 条）
反应条件
hydrogenchloride in ethanol
24 h; Ambient temperature;
参考文献
Kalvin, Douglas; Ramalingam, Kondareddiar; Woodward, Ronald
Synthetic Communications, 1985 , vol. 15, # 4 p. 267 - 272
参考文献
The Boots Company PLC
Patent: US5610161 A1, 1997 ;
反应条件
hydrogenchloride in diethyl ether
Ambient temperature; Yield given;
参考文献
Kotha; Kuki
Tetrahedron Letters, 1992 , vol. 33, # 12 p. 1565 - 1568
反应条件
1: 65.7 percent / KOH / ethanol / Ambient temperature
2: 85.7 percent / SOCl2 / toluene / Heating
3: NaN3 / H2O; acetone / 0 °C
4: benzene / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: 85.7 percent / SOCl2 / toluene / Heating
2: NaN3 / H2O; acetone / 0 °C
3: benzene / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: NaN3 / H2O; acetone / 0 °C
2: benzene / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: Ba(OH)2*8H2O / H2O / 160 °C
2: HCl / Heating
View Scheme
参考文献
Connors,T.A.; Ross,W.C.J.
Journal of the Chemical Society, 1960 , p. 2119 - 2132
反应条件
1: 77.8 percent / LiAlH4 / diethyl ether / Ambient temperature
2: 2.) NEt3 / 1.) 3 h, 0 deg C, ether, 2.) 20 h, r.t., ether
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
