in diethyl ether; ammonia byproducts: tolan; Ar atmosphere, addn. Et2O soln. of dibromostilbene to liq. NH3 soln. ofSn-compd. (-78°C); warming to room temp. (1 h), filtration (Ar atmosphere), removal ether;NMR;
参考文献
Mitchell, T. N.; Reinmann, W.
Organometallics, 1986 , vol. 5, p. 1991 - 1997
in tetrahydrofuran NaSnMe3 added to PhSnEt3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
Zavgorodnii, V. S.; Zubova, T. P.; Simin, V. B.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1765 - 1773
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 2048 - 2057
