1-(5-苯基噻吩-2-基)乙酮合成路线 （共 21 条）
反应条件
water; potassium carbonate in ethylene glycol dimethyl ether Substitution;
参考文献
Kotha, Sambasivarao; Kashinath, Dhurke; Lahiri, Kakali; Sunoj, Raghavan B.
European Journal of Organic Chemistry, 2004 , # 19 p. 4003 - 4013
反应条件
palladium diacetate; potassium carbonate in methanol Suzuki-Miyaura cross-coupling; 0.833333 h; Heating;
参考文献
Molander, Gary A.; Biolatto, Betina
Organic Letters, 2002 , vol. 4, # 11 p. 1867 - 1870
反应条件
tetrabutylammomium bromide; potassium carbonate in water T=120°C; Suzuki cross-coupling reaction; 0.25 h; Microwave irradiationsolid phase reaction;
参考文献
Bai, Lin; Wang, Jin-Xian
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 2 p. 315 - 320
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium acetate in 3,6,9,12,15,18,21,24,27-nonaoxanonacosane-1,29-diol T=100°C; Stille coupling; 1 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 9 p. 1378 - 1382
反应条件
4,5-dimethyl-3-(2-phenoxyphenyl)-1-(2,4,6-trimethylbenzyl)imidazolium chloride; palladium diacetate; caesium carbonate in 1,4-dioxane T=90°C; Suzuki-Miyaura Coupling; 18 h; Inert atmosphere;
参考文献
Kuriyama, Masami; Matsuo, Seira; Shinozawa, Mina; Onomura, Osamu
Organic Letters, 2013 , vol. 15, # 11 p. 2716 - 2719
反应条件
potassium carbonate; [Pd(C3H5)Cl]2/Tedicyp complex in xylene T=130°C; Suzuki reaction; 20 h;
参考文献
Kondolff, Isabelle; Doucet, Henri; Santelli, Maurice
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 1 p. 109 - 118
反应条件
phosphoric acid T=100°C; 2 - 14 h;
参考文献
Polyhedron, , vol. 54, p. 201 - 210
反应条件
tetrabutylammomium bromide; N-ethyl-N,N-diisopropylamine; palladium diacetate in xylene T=130°C; 118 h;
参考文献
Hassan, Jwanro; Hathroubi, Chokri; Gozzi, Christel; Lemaire, Marc
Tetrahedron, 2001 , vol. 57, # 37 p. 7845 - 7855
反应条件
tetrakis(triphenylphosphine) palladium(0); poly(ethylene glycol)-400; sodium acetate T=100°C; Stille cross-coupling; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 74, # 15 p. 5599 - 5602
反应条件
1: phenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-bromo-thien-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
