反应条件
1: 1,4-dibromonaphrthalene With isopropylmagnesium chloride; lithium chloride in tetrahydrofuran T=0 - 20°C; Grignard reaction; Inert atmosphereLarge scale reaction; 2: carbon dioxide in tetrahydrofuran T=-10 - 20°C; Large scale reaction;
参考文献
Harling, Sandra J.; Herbal, Karim; Langlade, Nathalie; Sanganee, Mahesh; Strachan, John B.; Turner, Peter G.; Whiting, Matthew P.; Bret, Guillaume; Loft, Mike; Negus, Alan; Shanahan, Steve
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 112 - 122