N-(苄氧基)邻苯二甲酰亚胺合成路线 （共 15 条）
反应条件
1: 2-hydroxy-1,3-isoindolinedione With sodium hydride in N,N-dimethyl-formamide Metallation; 2: benzyl bromide With sodium iodide in N,N-dimethyl-formamide T=70°C; Alkylation; 22 h;
参考文献
High; Prior; Bell; Rangachari
Journal of Pharmacology and Experimental Therapeutics, 1999 , vol. 288, # 2 p. 490 - 501
反应条件
[bis(acetoxy)iodo]benzene; copper(l) chloride in acetonitrile T=70°C; 12 h; Inert atmosphere;
参考文献
Ji, Min Lee; Eun, Ju Park; Seung, Hwan Cho; Chang, Sukbok
Journal of the American Chemical Society, 2008 , vol. 130, # 25 p. 7824 - 7825
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=25°C; 18 h;
参考文献
Kim, Sunggak; Lee, Tai Au; Song, Yukwan
Synlett, 1998 , # 5 p. 471 - 472
反应条件
sodium carbonate in water; N,N-dimethyl-formamide; acetonitrile 4 h;
参考文献
Uhlmann, Peter; Felding, Jakob; Vedso, Per; Begtrup, Mikael
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9177 - 9181
反应条件
triethylamine in N,N-dimethyl-formamide T=70°C; Condensation;
参考文献
Bartovic; Decroix; Netchitailo
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 4 p. 827 - 830
反应条件
ammonium cerium (IV) nitrate in water; acetone T=20 - 25°C; 0.666667 h; Inert atmosphere;
参考文献
Terent'ev, Alexander O.; Krylov, Igor B.; Sharipov, Mikhail Y.; Kazanskaya, Zoya M.; Nikishin, Gennady I.
Tetrahedron, 2012 , vol. 68, # 50 p. 10263 - 10271,9
反应条件
1: carbon monoxide With acetic acid 0.166667 h; 2: O-benzyl benzoylhydroxamic acid With palladium diacetate; p-benozquinone T=50 - 110°C; 18 h;
参考文献
Wrigglesworth, Joe W.; Cox, Brian; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2011 , vol. 13, # 19 p. 5326 - 5329
反应条件
1.1: potassium carbonate / water; ethyl acetate / 7 h / 0 - 20 °C 2.1: acetic acid / 0.17 h 2.2: 18 h / 50 - 110 °C View Scheme
参考文献
Wrigglesworth, Joe W.; Cox, Brian; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2011 , vol. 13, # 19 p. 5326 - 5329
反应条件
1.1: potassium carbonate / water; ethyl acetate / 7 h / 0 - 20 °C 2.1: acetic acid / 0.17 h 2.2: 18 h / 50 - 110 °C View Scheme
参考文献
Wrigglesworth, Joe W.; Cox, Brian; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2011 , vol. 13, # 19 p. 5326 - 5329
参考文献
Tanaka; Matsuo; Nakanishi; Kataoka; Takase; Otsuki
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 7 p. 2323 - 2330
