ethylaluminum dichloride in dichloromethane; toluene
T=-78 - 20°C; Yield given;
参考文献
Eissenstat, Michael A.; Bell, Malcolm R.; D'Ambra, Thomas E.; Alexander, E. John; Daum, Sol J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 16 p. 3094 - 3105
1: SOCl2, DMF / Ambient temperature
2: EtAlCl2 / CH2Cl2; toluene / -78 - 20 °C
View Scheme
参考文献
Eissenstat, Michael A.; Bell, Malcolm R.; D'Ambra, Thomas E.; Alexander, E. John; Daum, Sol J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 16 p. 3094 - 3105