1: 4-aminoacetophenone With hydrogenchloride; sodium nitrite in water
T=0°C; 0.0833333 h;
2: diphenyl diselenide in tetrahydrofuran; water
T=20°C; pH=7; Further stages. Title compound not separated from byproducts.;
1: diphenyl diselenide With hypophosphorous ether; glycerol in water
T=90°C; 0.5 h; Inert atmosphere;
2: alpha-chloropyridine in water
T=20°C; 2 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Thurow, Samuel; Webber, Rodrigo; Perin, Gelson; Lenardao, Eder J.; Alves, Diego
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3215 - 3218
