1: 95 percent / NaBH4 / ethanol / 18 h / 0 °C
2: 27.4 g / LiAlH4 / diethyl ether
3: 100 percent / toluene-p-sulphonic acid / CH2Cl2 / 1.5 h / Ambient temperature
View Scheme
参考文献
Kocienski, Philip; Yeates, Clive
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1879 - 1884
potassium tri-sec-butyl-borohydride in tetrahydrofuran
T=20°C; 3 h;
参考文献
Bowman, W. Russell; Fletcher, Anthony J.; Pedersen, Jan M.; Lovell, Peter J.; Elsegood, Mark R.J.; Hernandez Lopez, Elena; McKee, Vickie; Potts, Graeme B.S.
Tetrahedron, 2007 , vol. 63, # 1 p. 191 - 203