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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1666-96-2
合成路线
（共 81 条）
5332-24-1
3-溴喹啉
+
1078-58-6
二苯锌
→
反应条件
1666-96-2
反应条件
P(NC5H10)3; nickel dichloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.5 h;
参考文献
Gerber, Roman; Frech, Christian M.
Chemistry - A European Journal, 2011 , vol. 17, # 42 p. 11893 - 11904
79476-07-6
3-碘喹啉
+
383-35-7
→
反应条件
1666-96-2
反应条件
potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=100°C; 12 h;
参考文献
Hatanaka, Yasuo; Fukushima, Satoshi; Hiyama, Tamejiro
Heterocycles, 1990 , vol. 30, # 1 p. 303 - 306
5332-24-1
3-溴喹啉
→
反应条件
91-22-5
喹啉
+
1666-96-2
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=-30°C; 1 h;
参考文献
Quintin, Jerome; Franck, Xavier; Hocquemiller, Reynald; Figadere, Bruno
Tetrahedron Letters, 2002 , vol. 43, # 19 p. 3547 - 3549
5332-24-1
3-溴喹啉
+
100-59-4
苯基氯化镁
→
反应条件
91-22-5
喹啉
+
1666-96-2
反应条件
[polymer-incarcerated nickel nanocatalyst] PICB–NHC–Ni (0.25 mol percent as Ni) in tetrahydrofuran T=20°C; 12 h;
参考文献
Soule, Jean-Francois; Miyamura, Hiroyuki; Kobayashi, Shu
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10602 - 10605
79476-07-6
3-碘喹啉
+
23665-09-0
苯基碘化锌
→
反应条件
1666-96-2
反应条件
lithium chloride in tetrahydrofuran; toluene T=110°C; 48 h; Schlenk techniqueInert atmosphere;
参考文献
Shirakawa, Eiji; Tamakuni, Fumiko; Kusano, Eugene; Uchiyama, Nanase; Konagaya, Wataru; Watabe, Ryo; Hayashi, Tamio
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 521 - 525
Angew. Chem., 2014 , vol. 126, # 2 p. 531 - 535,5
5332-24-1
3-溴喹啉
+
108-86-1
溴代苯
→
反应条件
1666-96-2
反应条件
1: bromobenzene With (nBu)3MgLi in tetrahydrofuran; diethyl ether; hexane T=-30 - -10°C; 2: 3-(bromo)-quinoline With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane T=-10 - 20°C; 19 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron, 2003 , vol. 59, # 43 p. 8629 - 8640
5332-24-1
3-溴喹啉
+
591-50-4
碘苯
→
反应条件
1666-96-2
反应条件
1: 3-(bromo)-quinoline With (nBu)3MgLi in tetrahydrofuran; diethyl ether; hexane T=-30 - -10°C; 2: iodobenzene With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane T=-10 - 20°C; 19 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron, 2003 , vol. 59, # 43 p. 8629 - 8640
122-78-1
苯乙醛
+
74497-02-2
→
反应条件
1666-96-2
反应条件
trifluorormethanesulfonic acid; copper(I) bromide in dimethyl sulfoxide T=110°C; Catalytic behavior; Reagent/catalystSolventTemperature;
参考文献
Yan, Rulong; Liu, Xingxing; Pan, Congming; Zhou, Xiaoqiang; Li, Xiaoni; Kang, Xing; Huang, Guosheng
Organic Letters, 2013 , vol. 15, # 18 p. 4876 - 4879
108-86-1
溴代苯
→
反应条件
1666-96-2
反应条件
potassium hydroxide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide in tetrahydrofuran 8 h; Heating;
参考文献
Ishikura, Minoru; Oda, Izumi; Terashima, Masanao
Heterocycles, 1985 , vol. 23, # 9 p. 2375 - 2386
120-72-9
吲哚
→
反应条件
1666-96-2
反应条件
1: in dichloromethane cyclopropanation; 48 h; Heating; 2: With palladium on activated charcoal in toluene Rearrangement; 72 h; Heating;
参考文献
Rudler; Parlier; Durand-Reville; Martin-Vaca; Audouin; Garrier; Certal; Vaissermann
Tetrahedron, 2000 , vol. 56, # 28 p. 5001 - 5027
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