1: 3-chloropyridinetrifluoroborate With lithium diisopropyl amide in diethyl ether T=-78°C; Inert atmosphere; 2: 3-chloro-pyridine in diethyl ether T=-78°C; Inert atmosphere; 3: With water

1: With lithium diisopropyl amide in diethyl ether T=-78°C; Inert atmosphere; 2: With dimethyl-disulfide in diethyl ether Inert atmosphere; 3: With water

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a> <br />T=0&deg;C;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> <br /> &nbsp;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />&nbsp;ligand in CHCl2 was immersed in a stream of N2, to this BF3*Et2O was injected by syringe, top layer of etherate was frozen, reactor was allowed to warm slowly to room temp. with stirring for 10 h; solvent was removed in vac.; elem. anal.;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '2349612', constants.ctx, '0')">boron trifluoride diethyl etherate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=0&deg;C;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> &nbsp;