2′,4′,6′-三甲基苯乙酮合成路线 （共 135 条）
反应条件
1: With palladium (II) trifluoroacetate; 6-mbipy in water T=130°C; 1 h; Microwave irradiation; 2: With formic acid in water T=100°C; 1 h;
参考文献
Lindh, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Angewandte Chemie - International Edition, 2010 , vol. 49, # 42 p. 7733 - 7737
反应条件
titanium tetrachloride in dichloromethane T=-78 - 25°C; 2 h;
参考文献
Brook, Michael A.; Henry, Courtney
Tetrahedron, 1996 , vol. 52, # 3 p. 861 - 868
反应条件
1: TFA; Pd(OAc)2 / dimethylsulfoxide / 24 h / 80 °C 2: aq. TFA / dimethylsulfoxide / 2 h / 70 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 8 p. 2302 - 2303
反应条件
tetrachlorosilane; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane 24 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Suzuki, Kaoru
Chemistry Letters, 1992 , # 9 p. 1751 - 1754
反应条件
(1R)-N-oxyl-1-(N-benzylcarbamoyl)-8-azabicyclo[3.2.1]octane; sodium hydrogencarbonate; sodium bromide in dichloromethane; water T=0°C; Electrochemical reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Demizu, Yosuke; Shiigi, Hirofumi; Mori, Hiroyuki; Matsumoto, Kazuya; Onomura, Osamu
Tetrahedron Asymmetry, 2008 , vol. 19, # 23 p. 2659 - 2665
反应条件
ammonia; oxygen T=37.5°C; gaseous-phase reaction (atmospheric pressure) γ-radiolysis;
参考文献
Journal of the American Chemical Society, , vol. 102, # 9 p. 3120 - 3124
反应条件
cerium(III) chloride in tetrahydrofuran T=-50°C; 1.) 1 h, 2.) 3 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5295 - 5298
反应条件
methyloxirane in water; acetonitrile 6 h; Irradiation;
参考文献
Tetrahedron, , vol. 53, # 49 p. 16789 - 16794
反应条件
1: 91 percent / tetrahydrofuran / 2 h / 25 °C 2: 85 percent / pyridinium chlorochromate; SiO2 / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 16 p. 3577 - 3579
反应条件
2: dibutyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 64, p. 1450
Journal of the American Chemical Society, , vol. 66, p. 2135
