1,3,4-三苯基-4,5-二氢-1H-1,2,4-三氮唑-5-亚基合成路线 （共 7 条）
反应条件
T=80°C; P=0.08 Torr; 16 h;
参考文献
Enders, Dieter; Breuer, Klaus; Kallfass, Ulrike; Balensiefer, Tim
Synthesis, 2003 , # 8 p. 1292 - 1295
反应条件
1.1: SOCl2 / toluene / 7 h / 80 °C 2.1: 172 g / Et3N / tetrahydrofuran / 20 °C 3.1: acetic anhydride / 24 h / 20 °C 3.2: 141 g / NaOMe / 2 h / 20 °C 4.1: 100 percent / 24 h / 80 °C / 0.01 Torr View Scheme
参考文献
Synthesis, , # 8 p. 1292 - 1295
反应条件
1.1: 172 g / Et3N / tetrahydrofuran / 20 °C 2.1: acetic anhydride / 24 h / 20 °C 2.2: 141 g / NaOMe / 2 h / 20 °C 3.1: 100 percent / 24 h / 80 °C / 0.01 Torr View Scheme
参考文献
Synthesis, , # 8 p. 1292 - 1295
反应条件
1.1: acetic anhydride / 24 h / 20 °C 1.2: 141 g / NaOMe / 2 h / 20 °C 2.1: 100 percent / 24 h / 80 °C / 0.01 Torr View Scheme
参考文献
Synthesis, , # 8 p. 1292 - 1295
反应条件
1: With potassium tert-butylate; sodium hydride in THF-d8 (tetrahydrofuran-d8) Inert atmosphere; 2: With N,O-bis-(trimethylsilyl)-acetamide in THF-d8 (tetrahydrofuran-d8) Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 39 p. 7120 - 7124
参考文献
Journal of the American Chemical Society, , vol. 120, # 35 p. 9100 - 9101
参考文献
Enders, Dieter; Breuer, Klaus; Raabe, Gerhard; Runsink, Jan; Teles, J. Henrique; et al.
Angewandte Chemie, 1995 , vol. 107, # 9 p. 1119 - 1122
