1-乙基-1,2,3,4-四唑合成路线 (共 4 条)
反应条件
sodium azide; triethyl amine hydrochloride in N,N-dimethyl-formamide T=130°C; 4 h; Microwave irradiationInert atmosphere;
参考文献
Yoneyama, Hiroki; Usami, Yoshihide; Komeda, Seiji; Harusawa, Shinya
Synthesis (Germany), 2013 , vol. 45, # 8 art. no. SS-2013-F0025-OP, p. 1051 - 1059
反应条件
sodium hydroxide in water
3 h; Ambient temperature;
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Varyagina, L. G.; Zhigadlova, I. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 3 p. 341 - 343
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 3 p. 415 - 418
反应条件
sodium hydroxide in water
3 h; Ambient temperature;
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Varyagina, L. G.; Zhigadlova, I. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 3 p. 341 - 343
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 3 p. 415 - 418
反应条件
potassium carbonate in acetonitrile
18 h; Ambient temperature;
参考文献
Thomas, Edward W.; Cudahy, Michele M.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1623 - 1627