5-(4-硝基苯基)-1H-四唑合成路线 （共 29 条）
反应条件
acetic acid; sodium nitrite
参考文献
Justus Liebigs Annalen der Chemie, , vol. 298, p. 50
反应条件
hydrogen; palladium 10 on activated carbon in ethanol; ethyl acetate P=1551.49 Torr; 16 h;
参考文献
MERCK and CO., INC.
Patent: WO2006/15158 A1, 2006 ;
Location in patent: Page/Page column 38 ;
WO 2006/015158 A1
反应条件
sodium hydride in N,N-dimethyl-formamide T=5°C; 1.5 h;
参考文献
Spear, Robert J.
Australian Journal of Chemistry, 1984 , vol. 37, # 12 p. 2453 - 2468
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane T=25°C; 5 h; Product distribution;
参考文献
Osipova, T. F.; Ostrovskii, V. A.; Koldobskii, G. I.; Erusalimskii, G. B.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 357 - 362
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 398 - 404
反应条件
in 1,3,5-trimethyl-benzene T=160 - 170°C; 1 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 46, # 6 p. 1492 - 1494
参考文献
Chemische Berichte, , vol. 93, p. 2106 - 2124
反应条件
dicyclohexyl-carbodiimide in toluene
T=120°C; 0.25 h;
参考文献
Povazanec, Frantisek; Kovac, Jaroslav; Svoboda, Jozef
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 4 p. 1299 - 1300
反应条件
T=110°C; 0.5 h; Microwave irradiation;
参考文献
Efimova; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 9 p. 1345 - 1347
反应条件
in 1,3,5-trimethyl-benzene
T=160 - 170°C; 1 h;
参考文献
Uher, Michal; Foltin, Jozef; Povazanec, Frantisek; Kovac, Jaroslav
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 6 p. 1492 - 1494
反应条件
sodium hydroxide; tetrabutylammomium bromide
1) CH2Cl2, 25 deg C, 3 h, 2) 80 - 130 deg C; Yield given. Multistep reaction;
参考文献
Osipova, T. P.; Koldobskii, G. I.; Ostrovskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 1018 - 1019
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1119 - 1120
