5-(4-氯苯基)-1H-四唑合成路线 （共 12 条）
反应条件
sodium azide; copper(II) sulfate in dimethyl sulfoxide T=140°C; 0.5 h;
参考文献
Akhlaghinia, Batool; Rezazadeh, Soodabeh
Journal of the Brazilian Chemical Society, 2012 , vol. 23, # 12 p. 2197 - 2203
反应条件
sodium azide; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Patil, Umakant B.; Kumthekar, Kedar R.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3706 - 3709
反应条件
[bmim][N3]; hydroxylamine; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Heravi, Majid M.; Fazeli, Azadeh; Oskooie, Hossein A.; Beheshtiha, Yahya S.; Valizadeh, Hassan
Synlett, 2012 , vol. 23, # 20 p. 2927 - 2930
反应条件
sodium azide; tetrachlorosilane in acetonitrile T=20 - 82°C; 1.66667 h;
参考文献
El-Ahl, Abdel-Aziz S.; Amer, Fatty A.; Elbeheery, Akram H.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 11 p. 2226 - 2235
反应条件
triazidochlorosilane in acetonitrile 1.5 h; Heating;
参考文献
El-Ahl, Abdel-Aziz S.; Elmorsy, Saad S.; Elbeheery, Akram H.; Amer, Fathy A.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1257 - 1260
反应条件
in dimethylsulfoxide-d6; chloroform-d1 Equilibrium constant;
参考文献
Butler, Richard N.; Garvin, Victor C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 390 - 393
反应条件
in ethylene glycol dimethyl ether T=220°C; Huisgen reaction; P=8250.83 - 10501.1 Torr; 0.0833333 h; Microwave irradiationSealed vial;
参考文献
Reichart, Benedikt; Kappe, C. Oliver
Tetrahedron Letters, 2012 , vol. 53, # 8 p. 952 - 955
反应条件
in dimethylsulfoxide-d6; chloroform-d1 Equilibrium constant;
参考文献
Butler, Richard N.; Garvin, Victor C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 390 - 393
反应条件
in nitrobenzene
T=150°C; 2 h;
参考文献
Efimova, Yu. A.; Karabanovich; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 8 p. 1241 - 1244
反应条件
1: 75 percent / NaHCO3 / dimethylformamide / 0.5 h / 120 °C
2: 92 percent / dimethylformamide / 1 h / Heating
View Scheme
参考文献
Milcent, Rene; Barbier, Geo
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1233 - 1234
