N-叔丁基-3-酮-4-氮杂-5a-雄甾烯-17b-酰胺合成路线 （共 7 条）
反应条件
ammonium acetate in acetic acid 4 h; Heating;
参考文献
Xia, Peng; Yang, Zheng-Yu; Xia, Yi; Zhang, Hao-Bing; Zhang, Ke-Hua; Sun, Xun; Chen, Ying; Zheng, Yun-Qing
Heterocycles, 1998 , vol. 47, # 2 p. 703 - 716
反应条件
1: thionyl chloride / toluene; pyridine / 3 h / 5 °C 2: 0.5 h / 5 °C 3: 85.13 percent / NaIO4, KMnO4, Na2CO3 / 2-methyl-propan-2-ol; H2O / 0.5 h / Heating 4: 89.47 percent / ammonium acetate / acetic acid / 4 h / Heating View Scheme
参考文献
Heterocycles, , vol. 47, # 2 p. 703 - 716
反应条件
1: 85.13 percent / NaIO4, KMnO4, Na2CO3 / 2-methyl-propan-2-ol; H2O / 0.5 h / Heating 2: 89.47 percent / ammonium acetate / acetic acid / 4 h / Heating View Scheme
参考文献
Heterocycles, , vol. 47, # 2 p. 703 - 716
反应条件
1: 0.5 h / 5 °C 2: 85.13 percent / NaIO4, KMnO4, Na2CO3 / 2-methyl-propan-2-ol; H2O / 0.5 h / Heating 3: 89.47 percent / ammonium acetate / acetic acid / 4 h / Heating View Scheme
参考文献
Heterocycles, , vol. 47, # 2 p. 703 - 716
反应条件
1: 79.69 percent / 88percent HCOOH, K2CO3 / dimethylformamide / 6 h / Heating 2: 40.36 percent / <C6H5Se(O)>2O / chlorobenzene / 10 h / Heating View Scheme
参考文献
Xia, Peng; Yang, Zheng-Yu; Xia, Yi; Zhang, Hao-Bing; Zhang, Ke-Hua; Sun, Xun; Chen, Ying; Zheng, Yun-Qing
Heterocycles, 1998 , vol. 47, # 2 p. 703 - 716
反应条件
formic acid; potassium carbonate in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Xia, Peng; Yang, Zheng-Yu; Xia, Yi; Zhang, Hao-Bing; Zhang, Ke-Hua; Sun, Xun; Chen, Ying; Zheng, Yun-Qing
Heterocycles, 1998 , vol. 47, # 2 p. 703 - 716
反应条件
sodium tetrahydroborate; sulfuric acid in tetrahydrofuran 6 h; Ambient temperature; Yield given;
参考文献
Morzycki, Jacek W.; Wilczewska, Agnieszka Z.; Zochowska, Ewa; Lotowski, Zenon
Heterocycles, 1995 , vol. 41, # 12 p. 2729 - 2736
