1-(4-溴苯基)-3-苯基-1-丙酮合成路线 （共 8 条）
反应条件
(Ph)2SiH2; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) in chloroform 3 h; Ambient temperature;
参考文献
Keinan, Ehud; Greenspoon, Noam
Journal of the American Chemical Society, 1986 , vol. 108, # 23 p. 7314 - 7325
反应条件
1: With copper(I) bromide in tetrahydrofuran Heating / reflux; 2: With sulfuric acid in tetrahydrofuran; water
参考文献
WO2004/69792 A2, ;
Page 108-109 ;
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; silver carbonate in acetonitrile T=60°C; 24 h; regioselective reaction;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M. S.; Kommu, Nagaiah
European Journal of Organic Chemistry, 2012 , # 25 p. 4694 - 4698
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; silica gel in benzene T=70°C; 18 h;
参考文献
Yasui, Shinro; Fujii, Masayuki; Ohno, Atsuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4019 - 4026
反应条件
lithium tert-butylate in toluene T=110°C; 12 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
1: sodium hydroxide / ethanol / 4 h / 0 - 20 °C 2: acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II); butan-1-ol; potassium carbonate / 1 h / |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 14 p. 3690 - 3693
反应条件
diethyl ether anschliessend Behandeln mit wss. H2SO4;
参考文献
Journal of the American Chemical Society, , vol. 60, p. 1885,1888
反应条件
bromine in acetic acid
T=50°C;
参考文献
Orlov, V. D.; Insuasti, B.; Kolos, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 6 p. 685 - 687
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 6 p. 830 - 832
