环戊二烯-1,2,3,4,5-五羧酸戊甲酯合成路线 （共 7 条）
反应条件
in dichloromethane to benzene soln. decamethylstannocene added more acidic ligand (molar ratio 1:2), stirred for few days; recrystd. from CH3CN, elem. anal.;
参考文献
Kohl, Franz X.; Schlueter, Ewald; Jutzi, Peter
Journal of Organometallic Chemistry, 1983 , vol. 243, # 3 p. C37 - C38
反应条件
in benzene to benzene soln. decamethylstannocene added more acidic ligand (molar ratio 1:1); recrystd. from CH2Cl2, elem. anal.;
参考文献
Kohl, Franz X.; Schlueter, Ewald; Jutzi, Peter
Journal of Organometallic Chemistry, 1983 , vol. 243, # 3 p. C37 - C38
反应条件
hydrogenchloride; water
参考文献
Kelch, Andre S.; Jones, Peter G.; Dix, Ina; Hopf, Henning
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1705 - 1712
反应条件
T=100°C; 4 h; Yields of byproduct given;
参考文献
Jefferson, Elizabeth A.; Warkentin, John
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 463 - 467
反应条件
T=65°C; 2 h; Yields of byproduct given;
参考文献
Jefferson, Elizabeth A.; Warkentin, John
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 463 - 467
反应条件
1: Py / acetic acid; diethyl ether
2: aq. KOAc
View Scheme
参考文献
Le Goff,E.; LaCount,R.B.
Journal of Organic Chemistry, 1964 , vol. 29, p. 423 - 427
反应条件
0.333333 h; Ambient temperature;
参考文献
Jefferson, Elizabeth A.; Warkentin, John
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 463 - 467
