2-甲烷磺酰基-5-甲氧基嘧啶合成路线 （共 4 条）
反应条件
sodium hydroxide; water T=50°C; Hydrolysis;
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; Oxidation;
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
反应条件
1: 87 percent / POCl3; N,N-dimethylaniline / 2 h / Heating
2: 98 percent / Zn; NH4Cl; H2O / benzene / 8 h / Heating
3: 87 percent / MCPBA / CH2Cl2 / 20 °C
View Scheme
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
反应条件
1: 98 percent / Zn; NH4Cl; H2O / benzene / 8 h / Heating
2: 87 percent / MCPBA / CH2Cl2 / 20 °C
View Scheme
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
