3,6-二-2-吡啶基-1,2,4,5-四嗪合成路线 （共 9 条）
反应条件
nitric acid; acetic acid in water T=0°C;
参考文献
SUNG, Nack-do
Patent: WO2007/7943 A1, 2007 ;
Location in patent: Page/Page column 8 ;
反应条件
1: With hydrazine Inert atmosphereReflux; 2: With sodium nitrite in water; acetic acid T=0°C; 1 h; Inert atmosphere;
参考文献
Bakkali, Hicham; Marie, Cecile; Ly, Akarim; Thobie-Gautier, Christine; Graton, Jerome; Pipelier, Muriel; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Evain, Michel; Dubreuil, Didier
European Journal of Organic Chemistry, 2008 , # 12 p. 2156 - 2166
反应条件
acetic acid; sodium nitrite in water T=20°C;
参考文献
Chen, Weixuan; Wang, Danzhu; Dai, Chaofeng; Hamelberg, Donald; Wang, Binghe
Chemical Communications, 2012 , vol. 48, # 12 p. 1736 - 1738
反应条件
hydrazine hydrate; sodium nitrite 1.) room t., 48h; 2.) acetic acid, 0 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 22, # 15 p. 1393 - 1396
反应条件
in dichloromethane 0.333333 h; Inert atmosphereSchlenk technique;
参考文献
Chemical Communications, , vol. 49, # 66 p. 7325 - 7327
反应条件
Buckminsterfullerene in toluene T=25°C; 16 h;
参考文献
Chuang, Shih-Ching; Sander, Michael; Jarrosson, Thibaut; James, Scott; Rozumov, Eugene; Khan, Saeed I.; Rubin, Yves
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 2716 - 2723
反应条件
in anhydrous butyl ether 12 h; Heating;
参考文献
Hales, Neil J.; Heaney, Harry; Hollinshead, John H.; Ley, Steven V.
Tetrahedron, 1995 , vol. 51, # 28 p. 7755 - 7776
反应条件
in n-butylmethyl ether Diels-Alder-retro-Diels-Alder; 2 h; Reflux;
参考文献
Bula, Rafael P.; Oppel, Iris M.; Bettinger, Holger F.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3538 - 3542
反应条件
in anhydrous butyl ether
6 h; Heating;
参考文献
Hales, Neil J.; Heaney, Harry; Hollinshead, John H.; Ley, Steven V.
Tetrahedron, 1995 , vol. 51, # 28 p. 7755 - 7776
