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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-甲基尿苷
合成路线
（共 18 条）
16710-13-7
6-甲基尿苷
→
反应条件
626-48-2
2,4-二羟基-6-甲基嘧啶
+
50-69-1
D-核糖
反应条件
sodium hydroxide T=90.1°C; various reagent concentration, decomposition to nonchromophoric products; Rate constantMechanism;
参考文献
Loennberg, Harri; Suokas, Pekka; Kaeppi, Rainer; Darzynkiewicz, Edward
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 798 - 805
16710-13-7
6-甲基尿苷
→
反应条件
626-48-2
2,4-二羟基-6-甲基嘧啶
+
50-69-1
D-核糖
反应条件
sodium hydroxide T=90.1°C; various reagent concentration, decomposition to nonchromophoric products; Rate constantMechanism;
参考文献
Loennberg, Harri; Suokas, Pekka; Kaeppi, Rainer; Darzynkiewicz, Edward
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 798 - 805
142682-83-5
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
water; trifluoroacetic acid T=0 - 20°C; 1 h;
参考文献
Shih, Yu-Chiao; Yang, Ya-Ying; Lin, Chun-Chi; Chien, Tun-Cheng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4027 - 4036
362-43-6
2’,3’邻异亚丙基尿苷
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: H2O / 1 h / Heating 2: acetonitrile / 0.25 h / Heating 3: 66 percent / Raney nickel / ethanol / 1.5 h / Heating 4: 86 percent / aq. formic acid / 1 h / Ambient temperature View Scheme
参考文献
Jones, Simon S.; Reese, Colin B.; Ubasawa, Aiko
Synthesis, 1982 , # 4 p. 259 - 260
6974-32-9
1-乙酰基-2,3,5-三苯甲酰氧基-1-beta-D-呋喃核糖
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: trimethylsilyl triflate / acetonitrile / 0.5 h / Ambient temperature 2: MeONa/MeOH / 12 h 3: trifluoroacetic acid / 12 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
638-13-1
4-疏基-6-甲基嘧啶-2(1h)-酮
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: NaOH / Ambient temperature 2: (NH4)2SO4 / 12 h / Heating 3: trimethylsilyl triflate / acetonitrile / 0.5 h / Ambient temperature 4: MeONa/MeOH / 12 h 5: trifluoroacetic acid / 12 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
16710-11-5
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: (NH4)2SO4 / 12 h / Heating 2: trimethylsilyl triflate / acetonitrile / 0.5 h / Ambient temperature 3: MeONa/MeOH / 12 h 4: trifluoroacetic acid / 12 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
25691-85-4
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: MeONa/MeOH / Ambient temperature 2: 67 percent / BBr3 / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
25589-18-8
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: (NH4)2SO4 / 12 h / Heating 2: trimethylsilyl triflate / acetonitrile / 2 h / Ambient temperature 3: MeONa/MeOH / Ambient temperature 4: 67 percent / BBr3 / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
1070994-34-1
→
反应条件
16710-13-7
6-甲基尿苷
反应条件
1: trimethylsilyl triflate / acetonitrile / 2 h / Ambient temperature 2: MeONa/MeOH / Ambient temperature 3: 67 percent / BBr3 / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Felczak, Krzysztof; Drabikowska, Alicja K.; Vilpo, Juhani A.; Kulikowski, Tadeusz; Shugar, David
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1720 - 1728
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