1,2:3,4-二-o-异亚丙基-6-硫代-a-d-吡喃葡萄糖合成路线 （共 6 条）
反应条件
sodium methylate in methanol T=20°C; Deacetylation; 0.0833333 h;
参考文献
Carbohydrate Research, , vol. 326, # 2 p. 81 - 87
反应条件
1: pyridine / 1 h / 20 °C 2: dimethylformamide / 10 h / 50 °C 3: LAH / tetrahydrofuran / 0.5 h / 0 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 27 p. 3598 - 3601
反应条件
sodium sulfide; sodium ethanolate 1.) EtOH, 50 deg C, 2.) DMF, reflux; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 4 p. 1339 - 1343
反应条件
1: tetrahydrofuran / 20 °C / |Inert atmosphere 2: lithium aluminium tetrahydride / diethyl ether / 1 h / -30 - 20 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 8012 - 8016
Angew. Chem., , vol. 125, # 31 p. 8170 - 8174,5
反应条件
1: 93 percent / conc. H2SO4 / 4 h / Ambient temperature 2: 75 percent / pyridine / Ambient temperature 3: 1.) sodium sulfide, EtONa / 1.) EtOH, 50 deg C, 2.) DMF, reflux View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 4 p. 1339 - 1343
反应条件
tert-butylisonitrile; boron trifluoride in toluene T=20°C;
参考文献
Benati, Luisa; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Strazzari, Samantha; Zanardi, Giuseppe
Angewandte Chemie - International Edition, 2004 , vol. 43, # 27 p. 3598 - 3601
