4-苄基-2,5-二氢呋喃-2-酮合成路线 （共 23 条）
反应条件
acetone 3 h; Irradiation;
参考文献
Muraoka, Osamu; Tanabe, Genzoh; Momose, Takefumi
Heterocycles, 1990 , vol. 31, # 9 p. 1589 - 1592
反应条件
1,4-diaza-bicyclo[2.2.2]octane in acetone 3 h; Irradiation;
参考文献
Muraoka, Osamu; Tanabe, Genzoh; Higachiura, Mie; Minematsu, Toshie; Momose, Takefumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1437 - 1444
反应条件
1,4-diaza-bicyclo[2.2.2]octane in methanol 24 h; Irradiation;
参考文献
Muraoka, Osamu; Tanabe, Genzoh; Higachiura, Mie; Minematsu, Toshie; Momose, Takefumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1437 - 1444
反应条件
1,4-diaza-bicyclo[2.2.2]octane 3 h; Irradiation;
参考文献
Muraoka, Osamu; Tanabe, Genzoh; Higachiura, Mie; Minematsu, Toshie; Momose, Takefumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1437 - 1444
反应条件
1,4-diaza-bicyclo[2.2.2]octane 24 h; Irradiation;
参考文献
Muraoka, Osamu; Tanabe, Genzoh; Higachiura, Mie; Minematsu, Toshie; Momose, Takefumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1437 - 1444
反应条件
Grubb's 2nd generation catalyst in 1,2-dichloro-ethane
10 h; Heating;
参考文献
Hughes, Gregory; Kimura, Masanari; Buchwald, Stephen L.
Journal of the American Chemical Society, 2003 , vol. 125, # 37 p. 11253 - 11258
反应条件
triethylamine; lithium chloride; palladium dichloride in tetrahydrofuran; N,N-dimethyl-formamide
1.) 25 dec C, 23 h, 2.) reflux, 1 h;
参考文献
Larock; Stinn; Kuo
Tetrahedron Letters, 1990 , vol. 31, # 1 p. 17 - 20
反应条件
sodium hydrogencarbonate in toluene
1 h; Heating;
参考文献
Kametani, Tetsuji; Katoh, Tadashi; Tsubuki, Masayoshi; Honda, Toshio
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 1 p. 61 - 66
反应条件
1: 1,4-Dihydroxy-2-butyne With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0)
2: With N-methyl-2-indolinone; tetrapropylammonium perruthennate
T=-78 - 23°C; 62 h;
3: benzyl bromide With tris(dibenzylideneacetone)dipalladium (0)
Stille coupling reaction; Further stages.;
参考文献
Kamlage; Sefkow; Pool-Zobel; Peter
Chemical Communications, 2001 , # 4 p. 331 - 332
反应条件
1: 66 percent / 2,6-lutidine / toluene / 20 °C
2: 79 percent / benzylidene-RuCl2(PCy3)(di-N,N'-Mes-imidazole) complex / 1,2-dichloro-ethane / 10 h / Heating
View Scheme
参考文献
Hughes, Gregory; Kimura, Masanari; Buchwald, Stephen L.
Journal of the American Chemical Society, 2003 , vol. 125, # 37 p. 11253 - 11258
