N,N,N'-三苯基联苯胺合成路线 (共 14 条)
反应条件
1: 68 percent / t-BuONa; DPPF / Pd2(dba)3 / toluene / 7 h / 100 °C 2: 84 percent / t-BuONa; DPPF / Pd2(dba)3 / toluene / 6 h / 100 °C View Scheme
参考文献
Macromolecules, , vol. 38, # 5 p. 1640 - 1647
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / -80 °C / Inert atmosphere 1.2: 15 h / -80 - 20 °C 2.1: potassium carbonate; tris-(o-tolyl)phosphine / palladium diacetate / toluene; ethanol; water / 10.5 h / 100 °C / Inert atmosphere View Scheme
反应条件
1: potassium carbonate / toluene; nitrobenzene; ethyl acetate 2: potassium carbonate; diphenylamine / toluene; nitrobenzene; 3-methyl-1-butanol; hexane View Scheme
反应条件
1: potassium carbonate / toluene; nitrobenzene; ethyl acetate 2: potassium carbonate; diphenylamine / toluene; nitrobenzene; 3-methyl-1-butanol; hexane View Scheme