反应条件
1: 4 g / 1) Pb(OAc)4 2) iodine / CCl4 / Heating; Irradiation 2: 1) KOAc/AcOH 2) aq.NaOH 3: H+ 4: 1) H+ 2) KMnO4/AcOH 3) H+ / acetone 5: pyridine 6: 1) Pb(OAc)4 2) I2 / Irradiation 7: 1) Zn/Hg/HCl 2) aq. NaOH / 1.) reflux, 5 h 2.) reflux, 3 h 8: H+ 9: 350 mg / LiAlH4 / tetrahydrofuran / 3 h / Heating 10: 200 mg / ethylorthoformate/benzoic acid, 3.) alc. KOH / 1.) 70-80 deg C, 1 h 2.) 170 deg C, 4 h 3.) reflux, 8 h 11: 100 mg / pyridine / 1 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 806 - 809
