(1S,2S)-N-(对甲苯磺酰)-1,2-二苯基乙二胺合成路线 (共 4 条)
反应条件
triethylamine in tetrahydrofuran T=20°C; 12 h; Cooling with ice;
参考文献
Li, Wenjun; Wu, Wenbin; Yu, Feng; Huang, Huicai; Liang, Xinmiao; Ye, Jinxing
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2505 - 2511
反应条件
sodium hydroxide; water in dichloromethane T=0°C; 2 h; Product distribution / selectivity;
参考文献
EP1375477 A2, ;
Page/Page column 7-8 ;
反应条件
triethylamine in dichloromethane T=20°C; 12 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 5 p. 787 - 797
反应条件
triethylamine in isopropyl alcohol T=80°C; 1 h;
参考文献
ELANCO ANIMAL HEALTH IRELAND LIMITED; Guillemont, Jerome Emile Georges; Raboisson, Pierre Jean-Marie Bernard; Lounis, Nacer
Patent: US2013/109694 A1, 2013 ;
Location in patent: Paragraph 0082-0083 ;