5-硝基吲哚-2-甲酸乙酯合成路线 (共 21 条)
反应条件
PPA in xylene T=110°C; 1 h;
参考文献
Synthesis, , # 3 p. 222 - 223
反应条件
copper(l) iodide in dimethyl sulfoxide T=50°C; 0.166667 h; Ionic liquidInert atmosphereMicrowave irradiationSealed tube;
参考文献
Journal of the Brazilian Chemical Society, , vol. 22, # 11 p. 2036 - 2039
反应条件
PPA T=50 - 60°C; 4 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 15 p. 4638 - 4644
反应条件
Bi(NO3)3; PPA in methanol 2.5 h; Reflux;
参考文献
Synthetic Communications, , vol. 39, # 14 p. 2506 - 2515
反应条件
1.2: KOH / ethanol; H2O 2.1: polyphosphoric acid View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 14 p. 2443 - 2446
反应条件
1: aq.-ethanolic KOH 2: copper (II)-oxide; quinoline View Scheme
参考文献
Parmerter et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 4621
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Cavallini; Ravenna
Farmaco, Edizione Scientifica, 1958 , vol. 13, p. 105,109
反应条件
ammonium formate; palladium on activated carbon in ethanol 0.5 h; Heating / reflux;
参考文献
WO2005/80367 A1, ;
Page/Page column 67-68; 113-114 ;
参考文献
US2011/224137 A1, ;
US 20110224137 A1
反应条件
1: aq.-ethanolic KOH 2: copper (II)-oxide; quinoline 3: platinum; ethanol / Hydrogenation View Scheme
参考文献
Cavallini; Ravenna
Farmaco, Edizione Scientifica, 1958 , vol. 13, p. 105,109
反应条件
1: H2 2: ethyl dimethylaminopropylcarbodiimide / dimethylformamide View Scheme
参考文献
Rajeswari; Adesomoju; Cava
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 3 p. 557 - 564