(3,4-二甲基苯基)硫脲合成路线 (共 3 条)
反应条件
1: bromine; S2cl2; chlorobenzene 2: aqueous KOH / 210 °C / und anschliessend mit Acetanhydrid und Essigsaeure 3: zinc-powder; acetic acid; acetic acid anhydride View Scheme
参考文献
Barany; Pianka
Journal of the Chemical Society, 1953 , p. 2217,2223
参考文献
Barany; Pianka
Journal of the Chemical Society, 1953 , p. 2217,2223
反应条件
ammonium hydroxide; bromine; acetic acid 1.) room temp. 2.) room temp.; Yield given. Multistep reaction;
参考文献
Kajino; Mizuno; Tawada; Shibouta; Nishikawa; Meguro
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 11 p. 2888 - 2895