(±)-2-氯-1-苯基乙醇合成路线 (共 94 条)
反应条件
1: AlCl3 / CS2 / 0.5 h / Heating 2: 78 percent / sodium cyanoborohydride; zinc iodide / CH2Cl2 / 16 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 34, # 5 p. 895 - 901
反应条件
sodium azide; halohydrin dehalogenase from Agrobacterium radiobacter AD1; isopropyl alcohol T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2293 - 2298
反应条件
in ethanol T=27°C; 2 h; Rhodotorula glutinis NRRL Y-1091, culture medium; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 33, # 48 p. 7337 - 7340
反应条件
in ethanol T=27°C; 24 h; Mucor racemosus, 0.2 M pH 6.0 potassium phosphate buffer; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 33, # 48 p. 7337 - 7340
反应条件
lithium chloride 312 h; Ambient temperature; Yields of byproduct given;
参考文献
Kotsuki, Hiyoshizo; Shimanouchi, Tomoyasu
Tetrahedron Letters, 1996 , vol. 37, # 11 p. 1845 - 1848
反应条件
bis(cyclopentadienyl)titanium dichloride; cyclohexa-1,4-diene Electrochemical reaction;
参考文献
Mendeleev Communications, , vol. 21, # 4 p. 194 - 195
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 198, p. 1430
Journal of the Chemical Society, , p. 114
反应条件
2,2'-azo-bisisobutyronitrile; triphenylstannane in methanol T=61°C; 96 h; other α-haloacetophenone; var. solvents, times; Product distributionRate constantMechanism;
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5182 - 5186
反应条件
in ethanol T=27°C; 24 h; Mucor racemosus, culture medium 2 L, other substrate, other microorganism, other time, other medium; Mechanism;
参考文献
Tetrahedron Letters, , vol. 33, # 48 p. 7337 - 7340
参考文献
Monatshefte fuer Chemie, , vol. 36, p. 6