反应条件
methyl iodide in tetrahydrofuran; pentane
byproducts: isobutane; inert atmosphere; addn. of t-BuLi in pentane to Ph2GeH2 in THF (Li:Ge=2.4:1, -40°C), stirring (-40°C, 40 min), addn. of excess MeI (15 min), then 20°C, 1 h; hydrolysis, extn., concentration (vac.);
参考文献
Castel; Riviere; Satge; Ko
Organometallics, 1990 , vol. 9, # 1 p. 205 - 210