N-苄氧羰酰基-L-丝氨酸甲酯合成路线 (共 40 条)
反应条件
α-chymotripsin on Celite; Tris buffer; TEA in acetonitrile T=30°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 39, # 9 p. 997 - 1000
反应条件
1: ethanol; hydrazine hydrate 2: acetic acid; aqueous HCl; NaNO2 / unter Kuehlung und Behandeln des gebildeten Azids mit Glycin-aethylester in Aethylacetat und Aether 3: aqueous methanol. NaOH View Scheme
参考文献
Fruton
Journal of Biological Chemistry, 1942 , vol. 146, p. 463,469
反应条件
subtilisin-CLEC in acetonitrile T=40°C; 28 h;
参考文献
Wang, Yi-Fong; Yakovlevsky, Kirill; Zhang, Bailing; Margolin, Alexey L.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3488 - 3495
反应条件
α-chymotripsin on Celite; Tris buffer; TEA in acetonitrile T=30°C; 48 h;
参考文献
Miyazawa, Toshifumi; Tanaka, Kayoko; Ensatsu, Eiichi; Yanagihara, Ryoji; Yamada, Takashi
Tetrahedron Letters, 1998 , vol. 39, # 9 p. 997 - 1000
反应条件
α-chymotrypsin immobilised on Celite; Tris buffer; triethylamine in acetonitrile T=30°C; pH=7.8; 48 h;
参考文献
Miyazawa, Toshifumi; Tanaka, Kayoko; Ensatsu, Eiichi; Yanagihara, Ryoji; Yamada, Takashi
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 1 p. 87 - 93
参考文献
Olsen; Severinsen; Rasmussen; Hentzer; Givskov; Nielsen
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 3 p. 325 - 328
反应条件
diisopropyl-carbodiimide; copper(l) chloride in acetonitrile T=40°C; 6 h;
参考文献
Miller, Marvin J.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3131 - 3132
反应条件
1: With 4-(N,N-dimethlyamino)pyridine in acetonitrile T=20°C; 2: With N,N,N',N'-tetramethylguanidine in acetonitrile Further stages.;
参考文献
Ferreira, Paula M. T.; Monteiro, Luis S.; Pereira, Goreti; Ribeiro, Liliana; Sacramento, Joana; Silva, Liseta
European Journal of Organic Chemistry, 2007 , # 35 p. 5934 - 5949
反应条件
triphenylphosphine; diethylazodicarboxylate in benzene 15 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 61, # 7 p. 2544 - 2546
反应条件
triphenylphosphine; diethylazodicarboxylate in benzene 15 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 61, # 7 p. 2544 - 2546