反应条件
1: 2,2-(2)H2-n-butyliodide With iodine; magnesium in diethyl ether
0.5 h; Inert atmosphereReflux;
2: carbon dioxide in diethyl ether
Inert atmosphere;
3: With hydrogenchloride in diethyl ether
T=20°C; Inert atmosphere;
参考文献
Bowen, Richard D.; Edwards, Howell G. M.; Farwell, Dennis W.; Morgan, Sara E
Journal of Raman Spectroscopy, 2010 , vol. 41, # 12 p. 1725 - 1734