N-苄基-2-苯基-4-哌啶酮合成路线 （共 8 条）
反应条件
L-Selectridereg; in tetrahydrofuran T=-78°C; Reduction; 1 h;
参考文献
Creswell, Mark W.; Bolton, Gary L.; Hodges, John C.; Meppen, Malte
Tetrahedron, 1998 , vol. 54, # 16 p. 3983 - 3998
反应条件
aluminum oxide; cerium(III) chloride; sodium iodide T=35°C; Michael addition; 24 h;
参考文献
Bartoli, Giuseppe; Bartolacci, Massimo; Giuliani, Arianna; Marcantoni, Enrico; Massaccesi, Massimo; Torregiani, Elisabetta
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 169 - 174
反应条件
1: 81 percent / Yb(OTf)3 / acetonitrile / 1 h 2: 48 percent / L-Selectride / tetrahydrofuran / 1 h / -78 °C View Scheme
参考文献
Creswell, Mark W.; Bolton, Gary L.; Hodges, John C.; Meppen, Malte
Tetrahedron, 1998 , vol. 54, # 16 p. 3983 - 3998
反应条件
1: 3.6 g / trimethyl orthoformate / 3 h 2: 81 percent / Yb(OTf)3 / acetonitrile / 1 h 3: 48 percent / L-Selectride / tetrahydrofuran / 1 h / -78 °C View Scheme
参考文献
Creswell, Mark W.; Bolton, Gary L.; Hodges, John C.; Meppen, Malte
Tetrahedron, 1998 , vol. 54, # 16 p. 3983 - 3998
反应条件
1: 3.6 g / trimethyl orthoformate / 3 h 2: 81 percent / Yb(OTf)3 / acetonitrile / 1 h 3: 48 percent / L-Selectride / tetrahydrofuran / 1 h / -78 °C View Scheme
参考文献
Creswell, Mark W.; Bolton, Gary L.; Hodges, John C.; Meppen, Malte
Tetrahedron, 1998 , vol. 54, # 16 p. 3983 - 3998
反应条件
1: 83 percent / zinc triflate; water / CH2Cl2 / 5 h / 20 °C 2: 75 percent / CeCl3*7H2O; NaI; neutral alumina / 24 h / 35 °C View Scheme
参考文献
Bartoli, Giuseppe; Bartolacci, Massimo; Giuliani, Arianna; Marcantoni, Enrico; Massaccesi, Massimo; Torregiani, Elisabetta
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 169 - 174
反应条件
1: 83 percent / zinc triflate; water / CH2Cl2 / 5 h / 20 °C 2: 75 percent / CeCl3*7H2O; NaI; neutral alumina / 24 h / 35 °C View Scheme
参考文献
Bartoli, Giuseppe; Bartolacci, Massimo; Giuliani, Arianna; Marcantoni, Enrico; Massaccesi, Massimo; Torregiani, Elisabetta
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 169 - 174
反应条件
solid-phase synthesis; Yield given. Multistep reaction;
参考文献
Barco, Achille; Benetti, Simonetta; De Risi, Carmela; Marchetti, Paolo; Pollini, Gian P.; Zanirato, Vinicio
Tetrahedron Letters, 1998 , vol. 39, # 41 p. 7591 - 7594
