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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯硼酸
合成路线
（共 423 条）
1679-18-1
4-氯苯硼酸
→
反应条件
106-39-8
4-溴氯苯
反应条件
N-bromosuccinmide in acetonitrile T=81°C; 8 h;
参考文献
Thiebes, Christoph; Prakash, G. K. Surya; Petasis, Nicos A.; Olah, George A.
Synlett, 1998 , # 2 p. 141 - 142
1679-18-1
4-氯苯硼酸
+
105-36-2
溴乙酸乙酯
→
反应条件
14062-24-9
对氯苯乙酸乙酯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); i-Pr2NPPh2; water; potassium carbonate in tetrahydrofuran T=65°C; 8 h; Inert atmosphere;
参考文献
Peng, Zhi-Yong; Wang, Jian-Ping; Cheng, Jiang; Xie, Xiao-Min; Zhang, Zhaoguo
Tetrahedron, 2010 , vol. 66, # 42 p. 8238 - 8241
593-60-2
溴乙烯
+
1679-18-1
4-氯苯硼酸
→
反应条件
1073-67-2
4-氯苯乙烯
+
2050-68-2
4,4'-二氯联苯
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran; methanol T=100°C; Suzuki coupling; 1 h;
参考文献
Lando, Vanusa R.; Monteiro, Adriano L.
Organic Letters, 2003 , vol. 5, # 16 p. 2891 - 2894
1679-18-1
4-氯苯硼酸
+
931-59-9
苯次磺酰氯
→
反应条件
13343-26-5
4-氯二苯硫醚
反应条件
Pd(2-[2-(benzylthio)phenyliminomethyl]-4-bromophenol-(H))Cl; potassium carbonate in N,N-dimethyl-formamide T=90°C; 5 h; Sealed tubeInert atmosphere;
参考文献
Gogoi, Prasanta; Kalita, Mukul; Barman, Pranjit
Synlett, 2014 , vol. 25, # 6 art. no. 47, p. 866 - 870
1679-18-1
4-氯苯硼酸
+
882-33-7
二苯二硫醚
→
反应条件
13343-26-5
4-氯二苯硫醚
反应条件
[2,2']bipyridinyl; copper(l) iodide in water; dimethyl sulfoxide T=100°C; 12 h;
参考文献
Taniguchi, Nobukazu
Synlett, 2006 , # 9 p. 1351 - 1354
591-50-4
碘苯
+
1679-18-1
4-氯苯硼酸
→
反应条件
13343-26-5
4-氯二苯硫醚
反应条件
1: (4-Chlorophenyl)-boronic acid With CuF2; sulfur in dimethyl sulfoxide T=100°C; Chan-Lam Coupling; 12 h; Inert atmosphere; 2: With sodium tetrahydroborate in dimethyl sulfoxide T=40°C; 5 h; Inert atmosphere; 3: iodobenzene in dimethyl sulfoxide T=100°C; 20 h; Inert atmosphere;
参考文献
Yu, Jin-Tao; Guo, Huan; Yi, Yuanqiuqiang; Fei, Haiyang; Jiang, Yan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 749 - 752
1679-18-1
4-氯苯硼酸
+
108-98-5
硫酚
→
反应条件
13343-26-5
4-氯二苯硫醚
反应条件
1,10-phenanthroline; tetra(n-butyl)ammonium hydroxide; water; oxygen; copper(II) sulfate in ethanol T=25°C; Chan-Lam type S arylation; 8 h;
参考文献
Xu, Hua-Jian; Zhao, Yong-Qiang; Feng, Teng; Feng, Yi-Si
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2878 - 2884
1679-18-1
4-氯苯硼酸
+
98-80-6
苯硼酸
→
反应条件
13343-26-5
4-氯二苯硫醚
反应条件
1: 3,4,5-trimethoxyphenylboronic acid With potassium ethylxanthate; copper(l) chloride in methanol 3 h; Inert atmosphereReflux; 2: (4-Chlorophenyl)-boronic acid With potassium hydroxide in methanol 9 h; Inert atmosphereReflux;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Synlett, 2011 , # 20 art. no. W18411ST, p. 3041 - 3045
1679-18-1
4-氯苯硼酸
→
反应条件
163837-57-8
(-)-4-氯-Alpha-苯基-苯甲胺
反应条件
1: potassium fluoride; tetrakis-(ethylene)-μ,μ'-dichlorodirhodium(I); (1R,4R,7R)-naphthalen-2-yl 7-isopropyl-5-methylbicyclo[2.2.2]octa-2,5-diene-2-carboxylate / toluene; water / 16 h / 35 °C / |Inert atmosphere; |Schlenk technique 2: pyridine; water / 16 h / |Reflux View Scheme
参考文献
Crampton, Rosemary H.; Fox, Martin; Woodward, Simon
Tetrahedron Asymmetry, 2013 , vol. 24, # 9-10 p. 599 - 605
1679-18-1
4-氯苯硼酸
+
98-88-4
苯甲酰氯
→
反应条件
2005-08-5
对氯苯基苯甲酸
反应条件
oxygen; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0) in anhydrous xylene T=60°C; P=760.051 Torr; 12 h;
参考文献
Chen, Jiuxi; Peng, Yong; Liu, Miaochang; Ding, Jinchang; Su, Weike; Wu, Huayue
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2117 - 2122
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