反应条件
1: cyclohexenon; (4-Chlorophenyl)-boronic acid With 2,9-dimethyl-1,10-phenanthroline; oxygen; palladium diacetate in N,N-dimethyl-formamide
T=20°C; Boron-Heck reaction; 16 h;
2: 3,4,5-trimethoxyphenylboronic acid With sodium hydroxide in N,N-dimethyl-formamide
T=90°C; Suzuki coupling; 6 h; Inert atmosphere;
参考文献
O'Neill, Justin; Yoo, Kyung Soo; Jung, Kyung Woon
Tetrahedron Letters, 2008 , vol. 49, # 51 p. 7307 - 7310
