反应条件
1: 87 percent / NaI / acetone / 48 h / Heating 2: 1.) 80percent NaH / 1.) DMF, mineral oil, 50 deg C, 30 min, 2.) 50 deg C, 2 h; 70 deg C, 18 h 3: 57 percent / CH2Cl2 / 72 h / Heating 4: 96 percent Chromat. / 0.5M EtONa / ethanol / 4 h / 20 °C / other temperature View Scheme
参考文献
Benedetti, Fabio; Fabrissin, Silvio; Rusconi, Alessandro; Stirling, Charles J. M.
Gazzetta Chimica Italiana, 1988 , vol. 118, # 4 p. 233 - 240
