Boc-O-苄基-D-苏氨醇合成路线 （共 3 条）
反应条件
sodium tetrahydroborate; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide 1.) THF, a) 0 deg C, b) RT, 2.) THF, EtOH, 0 deg C; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 5 p. 1369 - 1377
反应条件
1: 1.) NaH / 1.) DMF, -15 deg C, 2 h, 2.) DMF, RT, 5 h 2: 1.) N-hydroxysuccinimide, dicyclohexylcarbodiimide, 2.) NaBH4 / 1.) THF, a) 0 deg C, b) RT, 2.) THF, EtOH, 0 deg C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 5 p. 1369 - 1377
反应条件
1: 1.) NaH / 1.) DMF, -15 deg C, 2 h, 2.) DMF, RT, 5 h 2: 1.) N-hydroxysuccinimide, dicyclohexylcarbodiimide, 2.) NaBH4 / 1.) THF, a) 0 deg C, b) RT, 2.) THF, EtOH, 0 deg C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 5 p. 1369 - 1377
