3-甲氧基-2-环己烯-1-酮合成路线 (共 49 条)
反应条件
Fe(OTs)3 T=20°C; 4 h;
参考文献
Mansilla, Horacio; Afonso, Maria M.
Synthetic Communications, 2008 , vol. 38, # 15 p. 2607 - 2618
反应条件
hydrogenchloride in methanol T=20°C; 12 h;
参考文献
Van Der Klei, Anita; De Jong, Robertus L. P.; Lugtenburg, Johan; Tielens, Aloysius G. M.
European Journal of Organic Chemistry, 2002 , # 17 p. 3015 - 3023
反应条件
potassium hydroxide in 1,4-dioxane; water T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 5213
反应条件
trimethyl orthoformate T=80°C; P=6000480 Torr; 19 h;
参考文献
Synlett, , # 14 art. no. U13805ST, p. 2254 - 2256
反应条件
in toluene T=20 - 90°C; Inert atmosphere;
参考文献
WO2013/181741 A1, ;
Page/Page column 36 ;
反应条件
2,3-dimethyl-buta-1,3-diene; triphenylphosphine; niobium bromide; zinc T=80°C; 2 h;
参考文献
Jou, Der-Ching; Hsiao, Tsung-Yu; Wu, Ming-Yuan; Kong, Kwang-Cheng; Cheng, Chien-Hong
Tetrahedron, 1998 , vol. 54, # 7 p. 1041 - 1052
反应条件
1: hex-5-ynoic acid With oxalyl dichloride in dichloromethane 2.5 h; Inert atmosphere; 2: With indium(III) chloride in dichloromethane 3 h; Inert atmosphere; 3: methanol in dichloromethane 0.25 h; Inert atmosphere;
参考文献
Hylden, Anne T.; Uzelac, Eric J.; Ostojic, Zeljko; Wu, Ting-Ting; Sacry, Keely L.; Sacry, Krista L.; Xi, Lin; Jones, T. Nicholas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1323 - 1326
反应条件
potassium carbonate 1 h; Ambient temperature;
参考文献
Mphahlele, Malose J.; Modro, Tomasz A.
Journal of Organic Chemistry, 1995 , vol. 60, # 25 p. 8236 - 8240
反应条件
tert.-butylhydroperoxide; Rh2(OAc)3(5-phenyl-2,8-di-2-thienylanthyridine-H); potassium carbonate in dichloromethane T=20°C; 10 h; Catalytic behavior;
参考文献
Huang, Da-Wei; Lo, Ying-Hao; Liu, Yi-Hung; Peng, Shie-Ming; Liu, Shiuh-Tzung
Organometallics, 2013 , vol. 32, # 14 p. 4009 - 4015
反应条件
1: KOtBu / 2-methyl-propan-2-ol 2: CH2Cl2 / 6 h / Heating View Scheme
参考文献
European Journal of Organic Chemistry, , # 1 p. 189 - 202